反应条件
1.1: NaH / dimethylformamide / 2 h / 0 - 20 °C
1.2: dimethylformamide / 3 h / 0 - 20 °C
2.1: 90 percent / Pd(dba)2; 1,1'-bis(diphenylphosphino)ferrocene / tetrahydrofuran / 5 h / 65 °C
3.1: LiOH / H2O; methanol / 5 °C
4.1: AgNO3 / acetone / 24 h / 20 °C
View Scheme
参考文献
Bellina, Fabio; Ciucci, Donatella; Vergamini, Piergiorgio; Rossi, Renzo
Tetrahedron, 2000 , vol. 56, # 16 p. 2533 - 2545
