2-羟基对苯二甲酸二甲酯合成路线 （共 18 条）
反应条件
bubbling air in water T=20°C; 12 h; Irradiation; Product distribution;
参考文献
Chemistry Letters, , # 3 p. 197 - 198
参考文献
Wegscheider; Bittner
Monatshefte fuer Chemie, 1900 , vol. 21, p. 639
反应条件
methanol; sodium hydroxide
T=220 - 240°C; im geschlossenen Rohr;
参考文献
Baeyer; Tutein
Chemische Berichte, 1889 , vol. 22, p. 2183
反应条件
1: NaBH4 / methanol
2: MnO2 / ethyl acetate
View Scheme
参考文献
Inoue, Seiichi; Yanai, Takayoshi; Ando, Shinji; Nakazawa, Akinori; Honda, Kiyoshi; Hoshino, Yujiro; Asai, Tomoyuki
Journal of Materials Chemistry, 2005 , vol. 15, # 44 p. 4746 - 4752
反应条件
sodium tetrahydroborate in methanol
T=20°C; 1 h;
参考文献
Weinert, Emily E.; Dondi, Ruggero; Colloredo-Melz, Stefano; Frankenfield, Kristen N.; Mitchell, Charles H.; Freccero, Mauro; Rokita, Steven E.
Journal of the American Chemical Society, 2006 , vol. 128, # 36 p. 11940 - 11947
反应条件
hydrogenchloride; sodium borohydride in methanol; benzene
参考文献
Banyu Pharmaceutical Co., Ltd.
Patent: US4335250 A1, 1982 ;
反应条件
1: 88 percent / pyridine / 24 h
2: 61 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating
3: 58 percent / p-TosOH / toluene / 0.75 h
4: 83 percent / pyridinium chlorochromate, Al2O3 / toluene / 2 h
View Scheme
参考文献
Weinges, Klaus; Reinel, Ute; Maurer, Wolfgang; Gaessler, Norbert
Liebigs Annalen der Chemie, 1987 , p. 833 - 838
反应条件
1: sodium hydroxide; methanol / 220 - 240 °C / im geschlossenen Rohr
2: NaOH-solution
View Scheme
参考文献
Baeyer; Tutein
Chemische Berichte, 1889 , vol. 22, p. 2183
