1: 1,2,4,5,6-tetramethoxybenzene With n-butyllithium in tetrahydrofuran T=-78°C; Inert atmosphere; 2: carbon dioxide in tetrahydrofuran Inert atmosphere;

1.1: potassium carbonate / acetone / Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere 2.2: Inert atmosphere View Scheme

1.1: water; potassium hydroxide / tetrahydrofuran / Inert atmosphere 2.1: potassium carbonate / acetone / Inert atmosphere 3.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere 3.2: Inert atmosphere View Scheme

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / Inert atmosphere 2.1: water; potassium hydroxide / tetrahydrofuran / Inert atmosphere 3.1: potassium carbonate / acetone / Inert atmosphere 4.1: n-butyllithium / tetrahydrofuran / -78 °C / Inert atmosphere 4.2: Inert atmosphere View Scheme

potassium hydroxide; ethanol; dihydrogen peroxide

1: aluminium chloride; carbon disulfide 2: ethanolic KOH-solution View Scheme

暂无反应条件数据