benzeneseleninic anhydride in tetrahydrofuran
40 h; Ambient temperature;
参考文献
Barton, Derek H. R.; Lester, David J.; Ley, Steven V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1212 - 1217
Barton, Derek H. R.; Lester, David J.; Ley, Steven V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1212 - 1217
1.1: selenium / diethyl ether / 0.5 h / Reflux
1.2: Cooling with ice
2.1: sodium tetrahydroborate / ethanol / Inert atmosphere; Cooling with ice
2.2: 4 h / Inert atmosphere; Reflux
View Scheme
参考文献
Yu, Fabiao; Li, Peng; Li, Guangyue; Zhao, Guangjiu; Chu, Tianshu; Han, Keli
Journal of the American Chemical Society, 2011 , vol. 133, # 29 p. 11030 - 11033
in tetrahydrofuran
T=0°C; 0.333333 h; oxidation of ketone and aldehyde hydrazones, oximes, and semicarbazones, hydroxylamines, hydrazo-compounds; various times, temperatures; Product distribution;
参考文献
Barton, Derek H. R.; Lester, David J.; Ley, Steven V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1212 - 1217
Chierici; Passerini
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1953 , vol. <8> 15, p. 69,72
