1,1-二甲氧基庚烷-2-酮合成路线 (共 12 条)
反应条件
toluene-4-sulfonic acid in benzene
24 h; Ambient temperature;
参考文献
Yu, Yin; Chen, Guo-qiang; Zhu, Jun; Zhang, Xu-sheng; Chen, Shu-xin; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 8 p. 2239 - 2243
参考文献
Royals; Robinson
Journal of the American Chemical Society, 1956 , vol. 78, p. 4161,4162
参考文献
Henze; Carroll
Journal of the American Chemical Society, 1954 , vol. 76, p. 4580,4582
反应条件
1: sodium methylate; benzene
2: aqueous methanol. KOH-solution
View Scheme
参考文献
Royals; Robinson
Journal of the American Chemical Society, 1956 , vol. 78, p. 4161,4162
反应条件
1: ethanolic sodium ethylate
2: aqueous methanol. KOH-solution
View Scheme
参考文献
Henze; Carroll
Journal of the American Chemical Society, 1954 , vol. 76, p. 4580,4582
反应条件
hydrogenchloride in tetrahydrofuran
参考文献
Cuvigny,T.; Normant,H.
Synthesis, 1977 , p. 198 - 200
反应条件
1: (i) Li, Et2NH, HMPT, benzene, THF, (ii) /BRN= 1730909/
2: aq. HCl / tetrahydrofuran
View Scheme
参考文献
Cuvigny,T.; Normant,H.
Synthesis, 1977 , p. 198 - 200
反应条件
(NH4)2S2O8
2 h; Heating;
参考文献
Tiecco, M.; Testaferri, L.; Tingoli, M.; Bartoli, D.
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4523 - 4528
反应条件
(NH4)2S2O8; diphenyl diselenide
2 h; Heating;
参考文献
Tiecco, M.; Testaferri, L.; Tingoli, M.; Bartoli, D.
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4523 - 4528
反应条件
phosphoric acid
1.) CH3OH, room temp., 12 h, 2.) room temp.; Yield given. Multistep reaction;
参考文献
Verhe, R.; Courtheyn, D.; Kimpe, N. De; Buyck, L. De; Schamp, N.
Synthesis, 1982 , # 8 p. 667 - 670