2-苄基巯基-1H-喹唑啉-4-酮合成路线 （共 6 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=20°C; 12 h; Inert atmosphere;
参考文献
Sanchez, Ana I.; Martinez-Barrasa, Valentin; Burgos, Carolina; Vaquero, Juan J.; Alvarez-Builla, Julio; Terricabras, Emma; Segarra, Victor
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 8 p. 2370 - 2378
反应条件
sodium hydroxide in ethanol
T=20°C; 3 h;
参考文献
Mertens, Matthias D.; Pietsch, Markus; Schnakenburg, Gregor; Guetschow, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 18 p. 8966 - 8979
反应条件
potassium carbonate in neat (no solvent)
T=20°C; Green chemistry; SolventTemperatureTimeReagent/catalyst;
参考文献
Reddy, B. Srinivasa; Naidu; Dubey
Asian Journal of Chemistry, 2013 , vol. 25, # 5 p. 2644 - 2646
反应条件
potassium hydroxide in ethanol
参考文献
Yun, L. M.; Yangibaev, S.; Shakhidoyatov, Kh. M.; Alekseeva, V. Ya.; V'yunov, K. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 2 p. 214 - 216
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 2 p. 254 - 256
反应条件
1: thionyl chloride / 2 h / Reflux
2: 0.5 h / 20 °C
3: potassium hydroxide / ethanol / 0.5 h / 20 °C
View Scheme
参考文献
Li, Hui; Wang, Jin-Ping; Yang, Fan; Liu, Ting; Qiu, Wen-Wei; Li, Jing-Ya; Li, Jia; Tang, Jie
Heterocycles, 2012 , vol. 85, # 8 p. 1897 - 1911
反应条件
1: 0.5 h / 20 °C
2: potassium hydroxide / ethanol / 0.5 h / 20 °C
View Scheme
参考文献
Li, Hui; Wang, Jin-Ping; Yang, Fan; Liu, Ting; Qiu, Wen-Wei; Li, Jing-Ya; Li, Jia; Tang, Jie
Heterocycles, 2012 , vol. 85, # 8 p. 1897 - 1911
