4-甲基-3-吡啶羧酸乙酯 1-氧化物合成路线 （共 5 条）
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform
T=0 - 23°C; 19 h;
参考文献
Penning, Miriam; Christoffers, Jens
European Journal of Organic Chemistry, 2014 , vol. 2014, # 10 p. 2140 - 2149
反应条件
1.1: sulfuric acid / water / 17 h / 130 °C
1.2: 4 h / 80 °C
2.1: 3-chloro-benzenecarboperoxoic acid / chloroform / 19 h / 0 - 23 °C
View Scheme
参考文献
Penning, Miriam; Christoffers, Jens
European Journal of Organic Chemistry, 2014 , vol. 2014, # 10 p. 2140 - 2149
反应条件
1: 1.) chromium trioxide, sulphuric acid / 1.) 70 deg C, 2.) reflux, 2 h
2: hydrogen peroxide / acetic acid / 3.5 h / 100 °C
View Scheme
参考文献
Clarke, Kenneth; Goulding, John; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1501 - 1505
反应条件
1: hydrogen chloride (gas) / 4 h / Heating
2: hydrogen peroxide / acetic acid / 3.5 h / 100 °C
View Scheme
参考文献
Clarke, Kenneth; Goulding, John; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1501 - 1505
反应条件
1: 2.2 g / 3 h / 100 °C
2: 76 percent / ethyl mercaptoacetate, sodium ethoxide / ethanol / 0.5 h / Heating
View Scheme
参考文献
Clarke, Kenneth; Goulding, John; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1501 - 1505
