反应条件
1.1: catecholborane; [Rh(COD)2](1+)BF4(1-); (S)-(-)-2,2'-bis(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxy-ethane / 8 h / -62 - -60 °C 1.2: 1,2-dimethoxy-ethane / -66 - 20 °C 2.1: n-BuLi / hexane; tetrahydrofuran / 0.17 h / -100 °C 2.2: ZnCl2 / hexane; tetrahydrofuran; diethyl ether / -100 - 20 °C 3.1: aq. NaClO2; amylene; potassium hydrogen phosphate / 2-methyl-propan-2-ol / 24 h / 20 °C View Scheme
参考文献
Chen, Austin; Ren, Li; Crudden, Cathleen M.
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9704 - 9710
