1-(环丙基羰基)-4-哌啶酮合成路线 (共 4 条)
反应条件
dimethyl sulfoxide; triethylamine in anhydrous dichloroethane; dichloromethane; water
参考文献
Eisai Co., Ltd.
Patent: US5221671 A1, 1993 ;
US 5221671 A
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine Swern oxidation;
参考文献
Fujita, Masakazu; Seki, Taketsugu; Inada, Haruaki; Ikeda, Naoko
Bioorganic and medicinal chemistry letters, 2002 , vol. 12, # 12 p. 1607 - 1611
反应条件
1: 95 percent / Et3N / CH2Cl2 / -60 °C 2: 72 percent / (COCl)2; Et3N; DMSO View Scheme
参考文献
Bioorganic and medicinal chemistry letters, , vol. 12, # 12 p. 1607 - 1611
反应条件
sodium hydroxide; potassium carbonate in tetrahydrofuran; water
参考文献
Merck and Co., Inc.
Patent: US4031222 A1, 1977 ;