2-乙基-N-甲基苯甲酰胺合成路线 （共 5 条）
反应条件
[2,2']bipyridinyl; bis(acetylacetonate)nickel(II) in 1,4-dioxane
T=95°C; 16 h; Inert atmosphere;
参考文献
Havlik, Sarah E.; Simmons, Jessica M.; Winton, Valerie J.; Johnson, Jeffrey B.
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3588 - 3593
反应条件
N,N'-dimethyl-N,N'-propyleneurea; cobalt(II) 2,4-pentanedionate in tetrahydrofuran
T=25°C; 12 h; Inert atmosphere;
参考文献
Chen, Quan; Ilies, Laurean; Yoshikai, Naohiko; Nakamura, Eiichi
Organic Letters, 2011 , vol. 13, # 12 p. 3232 - 3234
反应条件
N,N'-dimethyl-N,N'-propyleneurea; cobalt(II) 2,4-pentanedionate in tetrahydrofuran
T=25°C; 12 h; Inert atmosphere;
参考文献
Chen, Quan; Ilies, Laurean; Yoshikai, Naohiko; Nakamura, Eiichi
Organic Letters, 2011 , vol. 13, # 12 p. 3232 - 3234
反应条件
1: thionyl chloride; triethylamine / tetrahydrofuran / 0.33 h / 20 °C
2: 1.9 g / tetrahydrofuran / 2 h
View Scheme
参考文献
Lehmann, Fredrik; Currier, Erika A.; Olsson, Roger; Hacksell, Uli; Luthman, Kristina
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 8 p. 3057 - 3068
反应条件
in tetrahydrofuran
2 h;
参考文献
Lehmann, Fredrik; Currier, Erika A.; Olsson, Roger; Hacksell, Uli; Luthman, Kristina
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 8 p. 3057 - 3068
