2-氨基-5-氯苯甲酸合成路线 （共 147 条）
反应条件
hydrogen; palladium on activated charcoal in methanol P=735.5 Torr; 2 h; Ambient temperature;
参考文献
Polivka; Jilek; Holubek; et al.
Collection of Czechoslovak Chemical Communications, 1984 , vol. 49, # 1 p. 86 - 109
反应条件
sulfuryl dichloride in diethyl ether Reflux;
参考文献
Sinha, Girish Kumar; Pandey, Bibhishan; Sinha, Alka
Oriental Journal of Chemistry, 2010 , vol. 26, # 4 p. 1401 - 1406
反应条件
boron trifluoride diethyl etherate; sodium iodide in acetonitrile T=20°C; 0.583333 h;
参考文献
Kamal, Ahmed; Shankaraiah; Markandeya; Reddy, Ch. Sanjeeva
Synlett, 2008 , # 9 p. 1297 - 1300
反应条件
1: With sodium N-bromobenzenesulfonamide; sodium hydroxide; palladium dichloride in water; acetonitrile T=60°C; pH=12; 3.66667 h; 2: in water Acidic conditions;
参考文献
Karthikeyan; Jagadeesh, Rajenahally V.; Sree Sandhya; Puttaswamy; Nithya; Kumar, S. Senthil; Bhagat
Applied Organometallic Chemistry, 2011 , vol. 25, # 1 p. 34 - 46
反应条件
hydrogenchloride; dihydrogen peroxide in water; N,N-dimethyl-formamide T=45 - 50°C; 15 h;
参考文献
Borodina
Journal of applied chemistry of the USSR, 1986 , vol. 59, # 5 pt 2 p. 1087 - 1089
反应条件
1: With copper(l) iodide; sodium azide; ethanol; caesium carbonate T=20 - 95°C; Inert atmosphereSealed tube; 2: With hydrogenchloride in water pH=2 - 3;
参考文献
Zhao, Haibo; Fu, Hua; Qiao, Renzhong
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3311 - 3316
反应条件
sodium hydroxide 1 h; Heating;
参考文献
Okabe; Sun
Tetrahedron, 1995 , vol. 51, # 7 p. 1861 - 1866
反应条件
dihydrogen peroxide; sodium hydroxide in water
参考文献
Journal of Heterocyclic Chemistry, , vol. 47, # 2 p. 415 - 420
反应条件
1: hydrogenchloride / water / 4 h / |Reflux 2: Pseudomonas fluorescens kynureninase / aq. phosphate buffer / 37 °C / pH 8 / |Enzymatic reaction View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 21, # 15 p. 4670 - 4677
反应条件
1: N-chloro-succinimide; hydrogenchloride / acetic acid / 1 h / 20 °C 2: hydrogenchloride / water / 4 h / |Reflux 3: Pseudomonas fluorescens kynureninase / aq. phosphate buffer / 37 °C / pH 8 / |Enzymatic reaction View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 21, # 15 p. 4670 - 4677
