1,2,3,4-四氢喹啉合成路线 （共 372 条）
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in diethyl ether; cyclohexane T=25°C; 24 h; Inert atmosphere;
参考文献
Truong, Thanh; Daugulis, Olafs
Organic Letters, 2012 , vol. 14, # 23 p. 5964 - 5967
反应条件
copper diacetate; triethylamine in dichloromethane T=40°C; Ullmann condensation; 6 h; In air;
参考文献
Qin, Weiwei; Kakusawa, Naoki; Wu, Yichen; Yasuike, Shuji; Kurita, Jyoji
Chemical and Pharmaceutical Bulletin, 2009 , vol. 57, # 4 p. 436 - 438
参考文献
Omar-Amrani, Rafik; Schneider, Raphael; Fort, Yves
Synthesis, 2004 , # 15 p. 2527 - 2534
反应条件
1: palladium 10 on activated carbon / 24 h / 150 °C / Autoclave 2: palladium 10 on activated carbon; zinc / 100 °C / Autoclave View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 9 p. 1826 - 1833
反应条件
hydrogen; sulfided NiMo-Al2O3 in n-heptane T=349.9°C; P=52504.2 Torr; 2 h; Further byproducts given;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 11 p. 801 - 806
反应条件
hydrogen; aluminum oxide; nickel molybdenum in decane T=349.9°C; P=52504.2 Torr;
参考文献
Perot, G.; Brunet, S.; Canaff, C.; Toulhoat, H.
Bulletin des Societes Chimiques Belges, 1987 , vol. 96, # 11-12 p. 865 - 870
反应条件
1: palladium 10 on activated carbon / 24 h / 150 °C / Autoclave 2: palladium 10 on activated carbon; zinc / water; isopropyl alcohol / 40 h / 150 °C / Autoclave View Scheme
参考文献
Abarca, Belen; Adam, Rosa; Ballesteros, Rafael
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 9 p. 1826 - 1833
反应条件
hydrogen; sulfided NiMo-Al2O3 in n-heptane T=349.9°C; P=52504.2 Torr; 2 h; effect of the partial pressure of title compound; reaction in the presence of 2,6-diethylaniline; Product distributionMechanism;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 11 p. 801 - 806
反应条件
hydrogen; nickel T=210°C; P=7600 Torr; or 200 deg C, or Ru/C, 100 or 10 atm, 150 deg C, and competitive hydrogenation with 1,2,3,4-tetrahydroisoquinoline; Rate constant;
参考文献
Okazaki, Hiroshi; Onishi, Kiyotaka; Soeda, Mahito; Ikefuji, Yoshio; Tamura, Ryuji; Mochida, Isao
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 11 p. 3167 - 3174
反应条件
hydrogen; nickel T=200°C; P=7600 Torr; 2 h; other reaction time; Product distribution;
参考文献
Okazaki, Hiroshi; Onishi, Kiyotaka; Soeda, Mahito; Ikefuji, Yoshio; Tamura, Ryuji; Mochida, Isao
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 11 p. 3167 - 3174
