1,2,3,4-四氢喹啉合成路线 (共 372 条)
反应条件
dibenzothiophene Kinetics;
参考文献
Gutierrez, Oliver Y.; Hrabar, Ana; Hein, Jennifer; Yu, Yanzhe; Han, Jinyi; Lercher, Johannes A.
Journal of Catalysis, 2012 , vol. 295, p. 155 - 168
反应条件
1: With sulfuric acid; nitric acid T=-10 - 10°C; 3.5 h; 2: With sodium carbonate in water T=0°C; pH=8 - 9;
参考文献
Ceccarelli, Simona M.; Chomienne, Odile; Mattei, Patrizio; Sander, Ulrike Obst
Patent: US2008/153805 A1, 2008 ;
Location in patent: Page/Page column 15 ;
反应条件
sulfuric acid; potassium nitrate T=0 - 25°C; 1 h;
参考文献
European Journal of Organic Chemistry, , # 8 p. 1504 - 1513
反应条件
sulfuric acid; potassium nitrate T=0 - 25°C; 1 h;
参考文献
European Journal of Organic Chemistry, , # 8 p. 1504 - 1513
反应条件
N-bromosuccinmide in tetrachloromethane T=20°C; 3 h;
参考文献
Marchand, Pascal; Puget, Alain; Le Baut, Guillaume; Emig, Peter; Czech, Michael; Guenther, Eckhard
Tetrahedron, 2005 , vol. 61, # 16 p. 4035 - 4041
反应条件
bromine in chloroform T=-78°C; 2 h;
参考文献
Sahin, Ayse; Cakmak, Osman; Demirtas, Ibrahim; Okten, Salih; Tutar, Ahmet
Tetrahedron, 2008 , vol. 64, # 43 p. 10068 - 10074
反应条件
1: 22 percent / collidine / various solvent(s) / 120 h / Heating 2: 100 percent / H2 / 5percent Pd/C / ethanol; benzene / 2844.3 Torr View Scheme
参考文献
Glamkowski; Chiang
Journal of Heterocyclic Chemistry, 1987 , vol. 24, # 3 p. 733 - 737
反应条件
(+/-)-BINAP; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate in toluene Buchwald-Hartwig reaction; Reflux;
参考文献
Buckley, Benjamin R.; Christie, Steven D. R.; Elsegood, Mark R. J.; Gillings, Claire M.; Page, Philip C. Bulman; Pardoe, William J. M.
Synlett, 2010 , # 6 p. 939 - 943
反应条件
1: KNO3 / sulfuric acid 2: 4-(N,N-dimethlyamino)pyridine / dichloromethane View Scheme
反应条件
2,3,5-trimethyl-pyridine in various solvent(s) 120 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, # 3 p. 733 - 737