1,2,3,4-四氢喹啉合成路线 （共 372 条）
反应条件
(+/-)-BINAP; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate in toluene Buchwald-Hartwig reaction; Reflux;
参考文献
Synlett, , # 6 p. 939 - 943
反应条件
1: tetrahydrofuran / 24 h / Ambient temperature 2: MgCl2 / 2-methoxy-ethanol; tetrahydrofuran / 6 h / 125 °C View Scheme
参考文献
Van Wijngaarden; Hamminga; Van Hes; Standaar; Tipker; Tulp; Mol; Olivier; De Jonge
Journal of Medicinal Chemistry, 1993 , vol. 36, # 23 p. 3693 - 3699
反应条件
hydrogen; sulfided NiMo-Al2O3 in n-heptane T=349.9°C; P=52504.2 Torr; 2 h;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 11 p. 801 - 806
反应条件
hydrogen; sulfided NiMo-Al2O3 in n-heptane T=349.9°C; P=52504.2 Torr; 2 h; Further byproducts given;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 11 p. 801 - 806
反应条件
hydrogen; platinum on silica T=200°C;
参考文献
Journal of Organic Chemistry, , vol. 49, # 16 p. 2875 - 2880
反应条件
hydrogen; nickel-tungsten T=350°C; P=63755.1 - 108759 Torr; 8 h; other temperature; Product distribution;
参考文献
Cerny, Mirko; Trka, Antonin
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 6 p. 1749 - 1758
反应条件
hydrogen; sulfided NiMo-Al2O3 in n-heptane T=349.9°C; P=52504.2 Torr; 2 h; effect of the partial pressure of title compound; reaction in the presence of 2,6-diethylaniline; Product distributionMechanism;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 11 p. 801 - 806
反应条件
hydrogen sulfide; hydrogen; nickel-tungsten T=350°C; P=13876.1 - 108759 Torr; 8 h; Product distribution;
参考文献
Cerny, Mirko; Trka, Antonin
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 6 p. 1749 - 1758
参考文献
Bamberger; Williamson
Chemische Berichte, 1894 , vol. 27, p. 1470
Full Text Show Details
Bamberger; Lengfeld
Chemische Berichte, 1890 , vol. 23, p. 1142
反应条件
1.1: 75 percent / tris(dibenzylideneacetone)dipalladium(0); 1,1'-bis(diphenylphosphono)ferrocene; sodium tert-butoxide / toluene / 24 h / 100 °C
2.1: POCl3 / 0 °C
2.2: 80 percent / 90 °C
View Scheme
参考文献
Jung, Byung-Jun; Lee, Jeong-Ik; Chu, Hye Yong; Do, Lee-Mi; Lee, Jaemin; Shim, Hong-Ku
Journal of Materials Chemistry, 2005 , vol. 15, # 25 p. 2470 - 2475
