1,2,3,4-四氢喹啉合成路线 (共 372 条)
反应条件
bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I) in tert-butyl methyl ether T=60°C; 12 h; Inert atmosphereGloveboxSealed tube;
参考文献
Konishi, Shota; Kawamorita, Soichiro; Iwai, Tomohiro; Steel, Patrick G.; Marder, Todd B.; Sawamura, Masaya
Chemistry - An Asian Journal, 2014 , vol. 9, # 2 p. 434 - 438
反应条件
sulfuric acid in water; glycerol T=140°C; 2 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 7 p. 2220 - 2233
反应条件
T=990°C; P=0.05 Torr; Further byproducts given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 20 p. 1087 - 1088
→
10343-99-4(4aR,8aR)-1,2,3,4,4a,5,6,7,8,8a-十氢喹啉
反应条件
hydrogen; silica gel; ruthenium in octane T=100°C; P=22501.8 Torr; 1 h; Product distribution; Further Variations:CatalystsSolventsother aromatic and heterocyclic compounds;
参考文献
Journal of Catalysis, , vol. 213, # 1 p. 47 - 62
反应条件
1: 1.) NaH / 1.) DME, ether, reflux, 1h, 2.) reflux, 3 h 2: H2 / 10percent Pd-C / methanol / 760 Torr / Ambient temperature View Scheme
参考文献
Synthesis, , # 6 p. 481 - 485
反应条件
hydrogenchloride; indium in water 2.5 h; Reflux;
参考文献
Heterocycles, , vol. 77, # 2 p. 1163 - 1170
反应条件
T=650°C; P=0.005 Torr;
参考文献
Abramovitch, Rudolph A.; Kress, Albert O.; McManus, Samuel P.; Smith, Maurice R.
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3114 - 3121
反应条件
hydrogen fluoride; SbF5 T=0°C; 0.166667 h;
参考文献
Chemical Communications, , vol. 48, # 47 p. 5877 - 5879
反应条件
1: copper(l) iodide; caesium acetate / dimethyl sulfoxide / 20 h / 90 °C / |Inert atmosphere 2: lithium triethylborohydride / tetrahydrofuran / 1.5 h / 0 °C View Scheme
参考文献
Organic Letters, , vol. 15, # 13 p. 3440 - 3443
参考文献
Journal of the American Chemical Society, , vol. 42, p. 1723