1: 1-hydroxyindan With iPr2NCHEt2; (-)-Tetramisole in tetrahydrofuran T=-78°C; 0.5 h; Molecular sieveInert atmosphereResolution of racemate; 2: triphenyl-silyl chloride in tetrahydrofuran T=-78°C; 1 h; Inert atmosphereResolution of racemate; optical yield given as percent eeenantioselective reaction;
2-acetyloxy-1-propene; lipase YS in di-isopropyl ether T=30°C; 7 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Naemura, Koichiro; Fukuda, Ritsuko; Konishi, Masayoshi; Hirose, Keiji; Tobe, Yoshito
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 10 p. 1253 - 1256
