3-氯苯基硼 酸片呐醇 酯合成路线 （共 15 条）
反应条件
[Ir(κ3-pyridine-2,6-dicarboxylato)(1-κ-4,5-η-cyclooct-4-en-1-ido)(pyridine)] in chlorobenzene byproducts: H2; under Ar; Ir complex (5.0 molpercent), C6H5Cl and B compd. stirred and heated at 120°C for 20 h; solvent removed under vac. at room temp.; detd. by (1)H NMR spectra; mixt. of meta and para isomers (72:28) obtained;
参考文献
Dalton Transactions, , vol. 40, # 33 p. 8429 - 8435
反应条件
1.1: tetrafluoroboric acid / water / 0.17 h / 0 °C 1.2: 1 h / 0 °C 1.3: 2.5 h / 20 °C / |Inert atmosphere 2.1: diethyl ether / 4 h / 20 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 6 p. 1083 - 1088
反应条件
C2F3O2(1-)*C21H34IrN4(1+) T=180°C; 0.5 h; Microwave irradiationNeat (no solvent);
参考文献
Green Chemistry, , vol. 11, # 10 p. 1610 - 1617
反应条件
copper(ll) bromide in methanol Heating;
参考文献
Synthesis, , # 4 art. no. M05304SS, p. 547 - 550
反应条件
caesium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; water
0.5 h; Heating / reflux;
参考文献
Bossenmaier, Birgit; Friess, Thomas; Juchem, Rolf; Kling, Lothar; Kolm, Irene; Krell, Hans-Willi; von Hirschheydt, Thomas; Voss, Edgar
Patent: US2007/32530 A1, 2007 ;
Location in patent: Page/Page column 27 ;
