(二苯基甲基)硫代乙酸乙酯合成路线 （共 18 条）
反应条件
sodium ethanolate in ethanol T=30 - 35°C; 4.25 h;
参考文献
WO2003/95423 A1, ;
Page/Page column 7 ;
反应条件
sulfuric acid Heating;
参考文献
Prisinzano, Thomas; Podobinski, John; Tidgewell, Kevin; Luo, Min; Swenson, Dale
Tetrahedron Asymmetry, 2004 , vol. 15, # 6 p. 1053 - 1058
反应条件
1: concentrated aqueous HCl 2: concentrated sulfuric acid View Scheme
参考文献
Acta Chemica Scandinavica (1947-1973), , vol. 2, p. 856,858
反应条件
zinc(II) iodide in dichloromethane 0.75 h; Ambient temperature; Yield given;
参考文献
Canadian Journal of Chemistry, , vol. 67, p. 1071 - 1076
反应条件
1.1: H2SO4; 2-propanol; aq. H2O2 / methanol / 20 °C 2.1: 62.1 g / NaOH; H2O / ethanol / 1 h / 20 °C 3.1: (R)-(+)-α-methylbenzylamine / H2O / Heating 3.2: 17.0 g / aq. HCl / pH 2 View Scheme
参考文献
Prisinzano, Thomas; Podobinski, John; Tidgewell, Kevin; Luo, Min; Swenson, Dale
Tetrahedron Asymmetry, 2004 , vol. 15, # 6 p. 1053 - 1058
反应条件
1.1: H2SO4; 2-propanol; aq. H2O2 / methanol / 20 °C 2.1: 62.1 g / NaOH; H2O / ethanol / 1 h / 20 °C 3.1: (R)-(+)-α-methylbenzylamine / H2O / Heating 3.2: 17.0 g / aq. HCl / pH 2 4.1: 65 percent / K2CO3 / acetone / Heating View Scheme
参考文献
Prisinzano, Thomas; Podobinski, John; Tidgewell, Kevin; Luo, Min; Swenson, Dale
Tetrahedron Asymmetry, 2004 , vol. 15, # 6 p. 1053 - 1058
参考文献
Dahlbom; Oesterberg
Acta Chemica Scandinavica (1947-1973), 1948 , vol. 2, p. 856,858
反应条件
1: sulfuric acid; dihydrogen peroxide / methanol; isopropyl alcohol / 2 h / 20 °C 2: sodium hydroxide / ethanol; water / 2 h / 20 °C 3: ammonium hydroxide / dichloromethane / 2 h / 20 °C View Scheme
参考文献
Jung, Jae-Chul; Lee, Yeonju; Son, Jee-Young; Lim, Eunyoung; Jung, Mankil; Oh, Seikwan
Molecules, 2012 , vol. 17, # 9 p. 10446 - 10458
反应条件
1: 92 percent / hydroxylamine hydrochloride; KOH / methanol / 0.25 h 2: 72 percent / aq. H2O2; acetic acid / 40 °C View Scheme
参考文献
Prisinzano, Thomas; Podobinski, John; Tidgewell, Kevin; Luo, Min; Swenson, Dale
Tetrahedron Asymmetry, 2004 , vol. 15, # 6 p. 1053 - 1058
反应条件
1: H2SO4; 2-propanol; aq. H2O2 / methanol / 20 °C 2: 62.1 g / NaOH; H2O / ethanol / 1 h / 20 °C View Scheme
参考文献
Jung, Jae-Chul; Lee, Yeonju; Son, Jee-Young; Lim, Eunyoung; Jung, Mankil; Oh, Seikwan
Molecules, 2012 , vol. 17, # 9 p. 10446 - 10458
