(二苯甲基亚磺酰)乙酸甲酯合成路线 （共 13 条）
反应条件
sodium hydrogencarbonate in water
参考文献
Laboratoire L. Lafon
Patent: US4927855 A1, 1990 ;
反应条件
dihydrogen peroxide in methanol; water T=30°C; Kinetics; Temperature;
参考文献
Yadav, Ganapati D.; Subramanian; Manyar, Haresh G.
Organic Process Research and Development, 2010 , vol. 14, # 3 p. 537 - 543
反应条件
sodium carbonate in water; acetone T=20°C; 21.5 h; Heating / reflux; Product distribution / selectivity;
参考文献
Cephalon France; Organisation De Synthese Mondiale Orsymonde
Patent: US2006/135621 A1, 2006 ;
Location in patent: Page/Page column 22 ;
反应条件
triethylamine in methanol T=28 - 35°C; 2.25 h; Product distribution / selectivity;
参考文献
Cephalon France; Organisation De Synthese Mondiale Orsymonde
Patent: US2006/135621 A1, 2006 ;
Location in patent: Page/Page column 18 ;
反应条件
hydrogenchloride in water 1 - 19 h; Heating / reflux; Product distribution / selectivity;
参考文献
WO2007/103221 A2, ;
Page/Page column 22 ;
反应条件
ammonia in methanol T=25°C; 13.1667 h; Industry scale; Conversion of starting material;
参考文献
Orsymonde (Organisation de synthese Mondiale)
Patent: EP1477476 A1, 2004 ;
Location in patent: Page 14 ;
反应条件
ammonia; ammonium chloride in water T=20°C; 17 h; Product distribution / selectivity;
参考文献
TEVA PHARMACEUTICAL INDUSTRIES LTD.; TEVA PHARMACEUTICALS USA, INC.
Patent: WO2007/103221 A2, 2007 ;
Location in patent: Page/Page column 22 ;
反应条件
ammonia in methanol T=25°C; 13.1667 h; Industry scale; Conversion of starting material;
参考文献
Orsymonde (Organisation de synthese Mondiale)
Patent: EP1477476 A1, 2004 ;
Location in patent: Page 14 ;
反应条件
ammonia; ammonium chloride in water T=20°C; 17 h; Product distribution / selectivity;
参考文献
TEVA PHARMACEUTICAL INDUSTRIES LTD.; TEVA PHARMACEUTICALS USA, INC.
Patent: WO2007/103221 A2, 2007 ;
Location in patent: Page/Page column 22 ;
反应条件
ammonia in methanol
T=25°C; 13.1667 h; Industry scale; Conversion of starting material;
参考文献
Orsymonde (Organisation de synthese Mondiale)
Patent: EP1477476 A1, 2004 ;
Location in patent: Page 14 ;
