1-氯-6,6-二甲基-2-庚稀-4-炔合成路线 （共 3 条）
反应条件
1: With sodium carbonate in water T=77 - 83°C; 6 - 8 h; Industry scale; 2: With hydrogenchloride in water; toluene T=20 - 25°C; pH=0.5 - 1.5; 0.333333 h; Industry scale; Product distribution / selectivity;
参考文献
Kaspi, Joseph; Arad, Oded; Friedman, Oded; Manascu, Iosef; Fizitzki, Tamir; Danon, Edna
Patent: US2006/4230 A1, 2006 ;
Location in patent: Page/Page column 6; 10-11 ;
反应条件
boron trichloride in hexane
T=20°C; Chlorination; 0.166667 h; Product distribution; Further Variations:ReagentsTemperaturesreaction time;
参考文献
Chou, Shan-Yen; Tseng, Chin-Lu; Chen, Shyh-Fong
Tetrahedron Letters, 2000 , vol. 41, # 20 p. 3895 - 3898
反应条件
potassium carbonate in water
T=60°C; 9 h;
参考文献
Kazakov; Golosov
Pharmaceutical Chemistry Journal, 2006 , vol. 40, # 8 p. 452 - 454
