三乙基-1,3,5-戊烷三羧酸酯合成路线 （共 13 条）
反应条件
1: sodium / benzene / 14 h / Heating 2: H2SO4 , H3PO4 , H2O / 6 h View Scheme
参考文献
Gutsche,C.D. et al.
Tetrahedron, 1968 , vol. 24, p. 859 - 876
反应条件
1: sodium / benzene / 14 h / Heating 2: H2SO4 , H3PO4 , H2O / 6 h 3: 15 g / H2SO4 View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. <B> 20, # 4 p. 339 - 340
反应条件
oxonium; sodium; hydrogen cation 1.) toluene, 3.) C6H6; Multistep reaction;
参考文献
Synthetic Communications, , vol. 14, # 10 p. 925 - 932
反应条件
1: sodium / benzene / 14 h / Heating 2: H2SO4 , H3PO4 , H2O / 6 h 3: 15 g / H2SO4 4: 11 g / p-toluene-sulphonic acid / benzene / Heating View Scheme
参考文献
Murthi, G. S. S.; Mazumder, Alok
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. <B> 20, # 4 p. 339 - 340
反应条件
sulfuric acid
Esterification; 96 h; Heating;
参考文献
Suissa, M. Rachel; Romming, Christian; Dale, Johannes
Chemistry - A European Journal, 1999 , vol. 5, # 10 p. 3055 - 3065
反应条件
1: 87 percent / HCl; H2O / 72 h / Heating
2: 83 percent / H2SO4 / 96 h / Heating
View Scheme
参考文献
Suissa, M. Rachel; Romming, Christian; Dale, Johannes
Chemistry - A European Journal, 1999 , vol. 5, # 10 p. 3055 - 3065
反应条件
acetic acid; zinc in methanol
参考文献
Huff,R. et al.
Helvetica Chimica Acta, 1977 , vol. 60, p. 907 - 921
反应条件
1: CuCl
2: Zn, AcOH / methanol
View Scheme
参考文献
Huff,R. et al.
Helvetica Chimica Acta, 1977 , vol. 60, p. 907 - 921
参考文献
Kay; Perkin
Journal of the Chemical Society, 1906 , vol. 89, p. 1647
反应条件
oxonium; hydrogen cation; N-benzyl-trimethylammonium hydroxide
1.) dioxan, 3.) C6H6; Multistep reaction;
参考文献
Ferrino, S. A.; Maldonado, L. A.
Synthetic Communications, 1984 , vol. 14, # 10 p. 925 - 932
