Demarcay
Annales de Chimie (Cachan, France), 1880 , vol. <5> 20, p. 462
Bulletin de la Societe Chimique de France, 1880 , vol. <2> 33, p. 524
Full Text Show Details
Walden
Chemische Berichte, 1891 , vol. 24, p. 2028
1: bromine / Behandeln dann mit alkoh.Kali
2: zinc; diluted sulfuric acid
View Scheme
参考文献
Demarcay
Annales de Chimie (Cachan, France), 1880 , vol. <5> 20, p. 462
Bulletin de la Societe Chimique de France, 1880 , vol. <2> 33, p. 524
Full Text Show Details
Walden
Chemische Berichte, 1891 , vol. 24, p. 2028
dilithium tetrachlorocuprate; 10-undecenylmagnesium chloride
1.) THF, Et2O, from -20 to -10 deg C, 2.) a) -20 deg C, 2 h, b) 25 deg C, 1 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mirviss, Stanley B.
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1948 - 1951