iodine in dichloromethane byproducts: (CH3)3SnI; stirring a soln. of educt and iodine for 2 h at -20°C; evapn. of solvent; addn. of CDCl3; not isolated; detected by (1)H-NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 373, p. 29 - 36
iodine in dichloromethane byproducts: (CH3)2SnClI; stirring a soln. of educt and iodine for 2 h at 20°C; evapn. of solvent; addn. of CDCl3; not isolated; detected by (1)H-NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 373, p. 29 - 36