您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-硝基碘苯
合成路线
（共 886 条）
636-98-6
4-硝基碘苯
+
40138-16-7
2-甲酰基苯硼酸
→
反应条件
924868-84-8
反应条件
Cl2Pd(Ph3P)2; sodium carbonate in water; dimethyl sulfoxide T=85°C; Suzuki-Miyaura coupling; 12 h; Inert atmosphere;
参考文献
Korich, Andrew L.; Hughes, Thomas S.
Organic Letters, 2008 , vol. 10, # 23 p. 5405 - 5408
636-98-6
4-硝基碘苯
→
反应条件
944-30-9
反应条件
1: 54 percent / dimethylformamide 2: 64 percent / CrO3 / 100 °C 3: 89 percent Chromat. / KF, tetraphenylphosphonium bromide / dimethylsulfoxide / 0.25 h / 130 °C View Scheme
参考文献
Beaumont, Andrew J.; Clark, James H.
Journal of Fluorine Chemistry, 1991 , vol. 52, # 3 p. 295 - 300
636-98-6
4-硝基碘苯
+
17933-03-8
3-甲基苯硼酸
→
反应条件
952-21-6
1-methyl-3-(4-nitrophenyl)benzene
反应条件
potassium carbonate; palladium diacetate in water; acetone Suzuki Coupling; 21 h; Heating / reflux;
参考文献
Codd, Ellen; Dax, Scott L.; Flores, Christopher; Jetter, Michelle; Youngman, Mark
Patent: US2006/223837 A1, 2006 ;
Location in patent: Page/Page column 29 ;
US 20060223837 A1
636-98-6
4-硝基碘苯
+
26919-48-2
→
反应条件
952-21-6
1-methyl-3-(4-nitrophenyl)benzene
反应条件
potassium acetate; palladium diacetate; N,N-dicyclohexylamine in N,N-dimethyl-formamide T=35°C; 2 h; Inert atmosphere;
参考文献
Rao, Maddali L.N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Tetrahedron Letters, 2010 , vol. 51, # 47 p. 6101 - 6104
636-98-6
4-硝基碘苯
+
937-01-9
三甲基(3-甲基苯基)锡烷
→
反应条件
612-75-9
3,3'-二甲基联苯
+
952-21-6
1-methyl-3-(4-nitrophenyl)benzene
反应条件
ArPdI(P(C6H5)3)2 in 1,2-dichloro-ethane T=120 - 130°C; 2 h;
参考文献
Kashin, N. A.; Bumagina, I. G.; Bumagin, N. A.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 1 p. 18 - 24
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 1 p. 21 - 28
636-98-6
4-硝基碘苯
+
625-95-6
3-碘甲苯
→
反应条件
952-21-6
1-methyl-3-(4-nitrophenyl)benzene
反应条件
copper in N,N-dimethyl-formamide 6 h; Heating;
参考文献
Shudo, Koichi; Ohta, Toshiharu; Okamoto, Toshihiko
Journal of the American Chemical Society, 1981 , vol. 103, # 3 p. 645 - 653
636-98-6
4-硝基碘苯
+
253342-48-2
→
反应条件
952-21-6
1-methyl-3-(4-nitrophenyl)benzene
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in N,N-dimethyl-formamide T=90°C; Suzuki-Miyaura Coupling; 24 h; Schlenk technique;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
636-98-6
4-硝基碘苯
+
937-01-9
三甲基(3-甲基苯基)锡烷
+
18115-61-2
→
反应条件
643-93-6
+
952-21-6
1-methyl-3-(4-nitrophenyl)benzene
反应条件
in dichloromethane T=120 - 130°C; P=0.001 Torr; 2 h; Product distributionMechanism;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 3 p. 411 - 417
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 3 p. 457 - 464
636-98-6
4-硝基碘苯
+
63503-60-6
→
反应条件
952-22-7
反应条件
potassium carbonate; sulfilimine based palladacycle in toluene T=110°C; Suzuki coupling; 2 h;
参考文献
Thakur, Vinay V.; Ramesh Kumar; Sudalai
Tetrahedron Letters, 2004 , vol. 45, # 14 p. 2915 - 2918
636-98-6
4-硝基碘苯
+
19093-37-9
→
反应条件
955-45-3
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene 2 h; Reflux;
参考文献
Bernoud, Ellse; Le Duc, Gaetan; Bantrell, Xavier; Prestat, Guillaume; Madec, David; Poll, Giovanni
Organic Letters, 2010 , vol. 12, # 2 p. 320 - 323
首页
上一页
1
...
71
72
73
74
75
76
77
...
89
下一页
末页
到第
页
确定
