4-氯-3-甲氧基-5-硝基苯羧酸甲酯合成路线 （共 4 条）
反应条件
oxalyl dichloride in N,N-dimethyl-formamide T=-20 - 80°C; 3 h;
参考文献
Wang, Lin; Gong, Jianxian; Deng, Lujiang; Xiang, Zheng; Chen, Zhixing; Wang, Yuefan; Chen, Jiahua; Yang, Zhen
Organic Letters, 2009 , vol. 11, # 8 p. 1809 - 1812
反应条件
1: 74 percent / HNO3, glacial acetic acid / acetic acid / 2 h / Ambient temperature 2: 88 percent / oxalyl chloride / dimethylformamide / -20 deg C; 80 deg C, 3 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 105, # 15 p. 5015 - 5024
反应条件
hydrogenchloride; iron in ethanol; water T=70°C; 3 h; Inert atmosphere;
参考文献
KING'S COLLEGE LONDON
Patent: US2012/149737 A1, 2012 ;
Location in patent: Page/Page column 89 ;
反应条件
1: 30 g / KOH / ethanol; H2O / 2 h / 80 °C
2: 60 percent / mercuric oxide, bromine / CCl4 / 5 h / Irradiation
View Scheme
参考文献
Meyers; Babiak; Campbell; et al.
Journal of the American Chemical Society, 1983 , vol. 105, # 15 p. 5015 - 5024
