10-烯丙基-2-氯-吩噻嗪合成路线 （共 7 条）
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in various solvent(s)
2 h; Ambient temperature;
参考文献
Gozlan; Ladkani; Halpern; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 2 p. 613 - 614
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in various solvent(s)
19 h; Ambient temperature;
参考文献
Gozlan; Ladkani; Halpern; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 2 p. 613 - 614
反应条件
sodium hydroxide in chlorobenzene; toluene
4.5 h; Heating; Yield given. Yields of byproduct given;
参考文献
Ivanov, P. Yu.; Bokanov, A. I.; Budanova, L. I.; Kuzovkin, V. A.; Shvedov, V. I
Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 9 p. 677 - 679
Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 9 p. 1119 - 1121
反应条件
1: benzyl-trimethyl-ammonium hydroxide
2: Raney nickel; dioxane / 108 - 116 °C / 33097.9 Torr / Hydrogenation.Behandeln des Reaktionsprodukts mit wss. Ameisensaeure und wss. Formaldehyd
3: CH3I; aq.-ethanolic NaOH
View Scheme
参考文献
Fujii
Yakugaku Zasshi, 1956 , vol. 76, p. 644,647, 648
Chem.Abstr., 1957 , p. 425
反应条件
1: Raney nickel; dioxane / 108 - 116 °C / 33097.9 Torr / Hydrogenation.Behandeln des Reaktionsprodukts mit wss. Ameisensaeure und wss. Formaldehyd
2: CH3I; aq.-ethanolic NaOH
View Scheme
参考文献
Fujii
Yakugaku Zasshi, 1956 , vol. 76, p. 644,647, 648
Chem.Abstr., 1957 , p. 425
反应条件
sodium hydroxide; methyl iodide
参考文献
Fujii
Yakugaku Zasshi, 1956 , vol. 76, p. 644,647, 648
Chem.Abstr., 1957 , p. 425
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane
23 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Gozlan; Ladkani; Halpern; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 2 p. 613 - 614
