2-氧代-3-苯基丙酸甲酯合成路线 （共 25 条）
反应条件
hydrogenchloride in tetrahydrofuran
0.5 h; Ambient temperature;
参考文献
Shin; Yonezawa; Yamada
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3934 - 3944
参考文献
Deol,B.S. et al.
Australian Journal of Chemistry, 1976 , vol. 29, p. 2459 - 2467
反应条件
methanol in hexane
T=0°C; 0.0833333 h;
参考文献
Hirose, Yayoi; Ohta, Emi; Kawai, Yasushi; Ohta, Shinji
Journal of Natural Products, 2013 , vol. 76, # 4 p. 554 - 558
反应条件
1: 77 percent / triethylamine / 1 h / Ambient temperature
2: 95 percent / 1 M HCl / tetrahydrofuran / 0.5 h / Ambient temperature
View Scheme
参考文献
Shin; Yonezawa; Yamada
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3934 - 3944
反应条件
1: 93 percent / thionyl chloride, acetyl chloride / 4 h / Ambient temperature
2: 77 percent / triethylamine / 1 h / Ambient temperature
3: 95 percent / 1 M HCl / tetrahydrofuran / 0.5 h / Ambient temperature
View Scheme
参考文献
Shin; Yonezawa; Yamada
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 10 p. 3934 - 3944
反应条件
hydrogenchloride in tetrahydrofuran
参考文献
De Luca, Lidia; Giacomelli, Giampaolo
Synlett, 2004 , # 12 p. 2180 - 2184
反应条件
1: 85 percent / trichloroisocyanuric acid / CH2Cl2 / 1 h / 15 - 20 °C
2: 95 percent / TEA / CH2Cl2 / 1.5 h / 25 °C
3: 1.0 g / aq. HCl / tetrahydrofuran
View Scheme
参考文献
De Luca, Lidia; Giacomelli, Giampaolo
Synlett, 2004 , # 12 p. 2180 - 2184
反应条件
1: 95 percent / TEA / CH2Cl2 / 1.5 h / 25 °C
2: 1.0 g / aq. HCl / tetrahydrofuran
View Scheme
参考文献
De Luca, Lidia; Giacomelli, Giampaolo
Synlett, 2004 , # 12 p. 2180 - 2184
反应条件
sulfuric acid in tetrahydrofuran; diethyl ether
Heating;
参考文献
Poisel,H.
Chemische Berichte, 1978 , vol. 111, p. 3136 - 3139
反应条件
1: (i) tBuOCl, (ii) /BRN= 3592982/
2: aq. H2SO4 / diethyl ether; tetrahydrofuran / Heating
View Scheme
参考文献
Poisel,H.
Chemische Berichte, 1978 , vol. 111, p. 3136 - 3139
