N-甲基-N-苯基萘-2-胺合成路线 (共 6 条)
反应条件
CM-phos; palladium diacetate; potassium carbonate; 3,4,5-trimethoxyphenylboronic acid in water
T=110°C; 24 h; Inert atmosphere;
参考文献
So, Chau Ming; Zhou, Zhongyuan; Lau, Chak Po; Kwong, Fuk Yee
Angewandte Chemie - International Edition, 2008 , vol. 47, # 34 p. 6402 - 6406
反应条件
potassium fluoride; 18-crown-6 ether; ammonium hydrogen carbonate in tetrahydrofuran
T=60°C; 12 h; Inert atmosphere;
参考文献
Bhojgude, Sachin Suresh; Kaicharla, Trinadh; Biju, Akkattu T.
Organic Letters, 2013 , vol. 15, # 21 p. 5452 - 5455
反应条件
sodium t-butanolate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride; chlorobis(triphenylphosphine)(1-naphthyl)nickel(II) in 1,4-dioxane
T=110°C; 0.5 h;
参考文献
Gao, Cai-Yan; Yang, Lian-Ming
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1624 - 1627
反应条件
NiCl(1-naphthyl)(PPh3)2; sodium hydride; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in 1,4-dioxane
T=110°C; Inert atmosphere;
参考文献
Huang, Jin-Hua; Yang, Lian-Ming
Organic Letters, 2011 , vol. 13, # 14 p. 3750 - 3753
反应条件
potassium hydroxide
Multistep reaction;
参考文献
Grellmann, K. H.; Schmitt, U.
Journal of the American Chemical Society, 1982 , vol. 104, # 23 p. 6267 - 6272
参考文献
Chem.Fabr.vorm.Sandoz
Patent: DE96402 ;