(S)-4,4'-二甲氧基-7,7'-二羟基-1,1'-螺双茚满合成路线 （共 3 条）
反应条件
copper(l) chloride in N,N-dimethyl-formamide
T=120°C; 12 h;
参考文献
Zhu, Shou-Fei; Fu, Yu; Xie, Jian-Hua; Liu, Bin; Xing, Liang; Zhou, Qi-Lin
Tetrahedron Asymmetry, 2003 , vol. 14, # 20 p. 3219 - 3224
反应条件
1: 98 percent / NaBr; glacial acetic acid; H2O2 / 24 h / 20 °C
2: 92 percent / BBr3 / CH2Cl2 / 12 h / -78 - 20 °C
3: 70 percent / CuCl / dimethylformamide / 12 h / 120 °C
View Scheme
参考文献
Zhu, Shou-Fei; Fu, Yu; Xie, Jian-Hua; Liu, Bin; Xing, Liang; Zhou, Qi-Lin
Tetrahedron Asymmetry, 2003 , vol. 14, # 20 p. 3219 - 3224
反应条件
1: 92 percent / BBr3 / CH2Cl2 / 12 h / -78 - 20 °C
2: 70 percent / CuCl / dimethylformamide / 12 h / 120 °C
View Scheme
参考文献
Zhu, Shou-Fei; Fu, Yu; Xie, Jian-Hua; Liu, Bin; Xing, Liang; Zhou, Qi-Lin
Tetrahedron Asymmetry, 2003 , vol. 14, # 20 p. 3219 - 3224
