2,5-环己二烯-1,4-二酮单肟合成路线 (共 96 条)
反应条件
1: With 3,6-bis(triphenylphosphonium)cyclohexene dichromate
T=20°C; 0.0833333 h;
2: With hydroxylamine
0.2 h;
参考文献
Badri, Rashid; Shushizadeh, Mohammad Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2007 , vol. 182, # 3 p. 601 - 605
反应条件
1: 92 percent / Fremy's salt, potassium hydrogen phosphate / methanol; H2O / 0.5 h
2: 42 percent / benzene / 6 h / Ambient temperature; Irradiation
View Scheme
参考文献
Baldry, Peter J.; Forrester, Alexander R.; Ogilvy, Munro M.; Thomson, Ronald H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 2027 - 2034
反应条件
silver(l) oxide in benzene
48 h; Further byproducts given;
参考文献
Baldry, Peter J.; Forrester, Alexander R.; Ogilvy, Munro M.; Thomson, Ronald H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 2027 - 2034
反应条件
in cyclohexane
6 h; Ambient temperatureIrradiation;
参考文献
Baldry, Peter J.; Forrester, Alexander R.; Ogilvy, Munro M.; Thomson, Ronald H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 2027 - 2034
反应条件
1: sulfomonoperoxoic acid
2: diluted sulfuric acid; methanol
View Scheme
参考文献
Baeyer; Knorr
Chemische Berichte, 1902 , vol. 35, p. 3036
反应条件
methanol; sulfuric acid
参考文献
Baeyer; Knorr
Chemische Berichte, 1902 , vol. 35, p. 3036
参考文献
Baeyer; Caro
Chemische Berichte, 1874 , vol. 7, p. 811
反应条件
hydroxylamine hydrochloride; water
参考文献
Goldschmidt
Chemische Berichte, 1884 , vol. 17, p. 216
Chemische Berichte, 1889 , vol. 22, p. 3107
反应条件
potassium phosphate buffer
T=37°C; half-life for the decomposition; Rate constant;
参考文献
Calder, Ian C.; Hart, Sandra J.; Healey, Kevin; Ham, Kathryn N.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 8 p. 988 - 993
反应条件
in benzene
6 h; Ambient temperatureIrradiation;
参考文献
Baldry, Peter J.; Forrester, Alexander R.; Ogilvy, Munro M.; Thomson, Ronald H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 9 p. 2027 - 2034