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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯乙烯
合成路线
（共 543 条）
10486-61-0
3-碘噻吩
+
637-69-4
4-甲氧基苯乙烯
→
反应条件
3172-56-3
3,3'-双噻吩
+
155827-34-2
反应条件
triethylamine in N,N-dimethyl-formamide T=90°C; Heck Reaction; 8 h; Solvent; Overall yield = 75 percent;
参考文献
Kamal, Ahmed; Srinivasulu, Vunnam; Seshadri; Markandeya, Nagula; Alarifi; Shankaraiah, Nagula
Green Chemistry, 2012 , vol. 14, # 9 p. 2513 - 2522
637-69-4
4-甲氧基苯乙烯
→
反应条件
3179-10-0
1-(4-甲氧苯基)-2-硝基乙烯
反应条件
TNM in acetonitrile 2 h; Irradiation;
参考文献
Mathew, Lizamma; Varghese, Babu; Sankararaman, S.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 12 p. 2399 - 2404
637-69-4
4-甲氧基苯乙烯
→
反应条件
3179-10-0
1-(4-甲氧苯基)-2-硝基乙烯
+
178101-25-2
反应条件
Nitrogen oxide in 1,2-dichloro-ethane T=22°C; P=1500.15 Torr; 3 h; Inert atmosphereAutoclave; regiospecific reaction;
参考文献
Jovel, Irina; Prateeptongkum, Saisuree; Jackstell, Ralf; Vogl, Nadine; Weckbecker, Christoph; Beller, Matthias
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 16 p. 2493 - 2497
637-69-4
4-甲氧基苯乙烯
+
572-09-8
乙酰溴-α-D-葡萄糖
→
反应条件
3947-62-4
2,3,4,6-四-O-乙酰-β-D-吡喃葡萄糖
反应条件
bis(1,5-cyclooctadiene)nickel (0); NH4Br; (R,R)-Ph-pybox; zinc in N,N-dimethyl acetamide T=25°C; 12 h; Inert atmosphere;
参考文献
Gong, Hegui; Andrews, R. Stephen; Zuccarello, Joseph L.; Lee, Stephen J.; Gagne, Michel R.
Organic Letters, 2009 , vol. 11, # 4 p. 879 - 882
637-69-4
4-甲氧基苯乙烯
+
64339-43-1
5-碘邻苯二酚
→
反应条件
65728-21-4
反应条件
C48H42Cl2O4P4Pd2; potassium carbonate in acetonitrile T=200°C; Heck reaction; P=20252 Torr; 0.333333 h; Microwave irradiation; regioselective reaction;
参考文献
Synthesis, , vol. 44, # 3 art. no. M89011SS, p. 446 - 452
637-69-4
4-甲氧基苯乙烯
→
反应条件
100-09-4
反应条件
1: With tert.-butylhydroperoxide; FeCl3*6H2O; sodium hydroxide in water T=80°C; 10 h; 2: With hydrogenchloride in water T=20°C;
参考文献
Shaikh, Tanveer Mahamadali; Hong, Fung-E
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 9 p. 1491 - 1496
637-69-4
4-甲氧基苯乙烯
→
反应条件
32345-64-5
+
100-09-4
反应条件
Oxonereg; in water; acetonitrile 24 h; Reflux; Time;
参考文献
Tetrahedron, , vol. 70, # 13 p. 2280 - 2285
637-69-4
4-甲氧基苯乙烯
→
反应条件
123-11-5
+
100-09-4
反应条件
Co(acetylacetonate)3; oxygen in tetrahydrofuran T=70°C; 36 h; Yield given. Yields of byproduct given;
参考文献
Reetz, Manfred T.; Toellner, Karl
Tetrahedron Letters, 1995 , vol. 36, # 52 p. 9461 - 9464
637-69-4
4-甲氧基苯乙烯
→
反应条件
18684-79-2
+
18684-94-1
+
100-09-4
+
2196-99-8
反应条件
chlorine dioxide in tetrachloromethane T=52 - 54°C; 1.16667 h; Further byproducts given;
参考文献
Polish Journal of Chemistry, , vol. 60, # 7-12 p. 811 - 824
637-69-4
4-甲氧基苯乙烯
→
反应条件
4136-21-4
反应条件
1.1: m-CPBA / H2O / 2 h / 20 °C 1.2: 15 percent / sulfuric acid / H2O / 2 h 2.1: 95 percent / 4-dimethylaminopyridine; triethylamine / CH2Cl2 / 20 °C 3.1: tetrapropylammonium perruthenate; N-methylmorpholine N-oxide / CH2Cl2 / 3 h / 20 °C 3.2: 386 mg / Oxone / H2O; methanol / 3 h / 20 °C View Scheme
参考文献
Tsujigami, Toshikuni; Sugai, Takeshi; Ohta, Hiromichi
Tetrahedron Asymmetry, 2001 , vol. 12, # 18 p. 2543 - 2549
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