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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-甲氧基苯乙烯
合成路线
（共 543 条）
3319-15-1
4-甲氧基-α-甲基苯甲醇
→
反应条件
637-69-4
4-甲氧基苯乙烯
反应条件
H3[PW12O40] in dimethyl sulfoxide T=100°C; 1 h; Inert atmosphere;
参考文献
Colbon, Paul; Barnard, Jonathan H.; Purdie, Mark; Mulholland, Keith; Kozhevnikov, Ivan; Xiao, Jianliang
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1395 - 1400
104-92-7
4-溴苯甲醚
→
反应条件
637-69-4
4-甲氧基苯乙烯
反应条件
caesium carbonate; triphenylphosphine; palladium dichloride in tetrahydrofuran; water T=85°C; Suzuki-Miyaura reaction; 22 h;
参考文献
Molander, Gary A.; Brown, Adam R.
Journal of Organic Chemistry, 2006 , vol. 71, # 26 p. 9681 - 9686
768-60-5
4-乙炔基苯甲醚
→
反应条件
637-69-4
4-甲氧基苯乙烯
+
1515-95-3
4-乙基苯甲醚
反应条件
hydrogen in hexane T=50°C; P=760.051 Torr; 10 h;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 5 p. 1481 - 1485
6303-59-9
1-((E)-2-溴乙烯基)-4-甲氧基苯
+
100-52-7
苯甲醛
→
反应条件
637-69-4
4-甲氧基苯乙烯
+
18684-94-1
4-甲氧基-反式-beta-氯苯乙烯
+
1346463-28-2
反应条件
copper(l) iodide; N,N-dimethylaminoacetic acid; [RuCl2Cp*]; caesium carbonate in N,N-dimethyl-formamide T=120°C; P=760.051 Torr; 4 h; Inert atmosphereSealed tube; Reagent/catalyst; stereoselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 134, # 40 p. 16468 - 16471,4
6303-59-9
1-((E)-2-溴乙烯基)-4-甲氧基苯
+
100-52-7
苯甲醛
→
反应条件
637-69-4
4-甲氧基苯乙烯
+
18684-94-1
4-甲氧基-反式-beta-氯苯乙烯
+
1346463-28-2
+
136618-41-2
反应条件
copper(l) iodide; N,N-dimethylaminoacetic acid; [RuCl2Cp*]; caesium carbonate; potassium iodide in N,N-dimethyl-formamide T=120°C; P=760.051 Torr; 4 h; Inert atmosphereSealed tube; Reagent/catalystTemperature; stereoselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 134, # 40 p. 16468 - 16471,4
108-05-4
醋酸乙烯酯
+
104-92-7
4-溴苯甲醚
→
反应条件
637-69-4
4-甲氧基苯乙烯
反应条件
[2,2']bipyridinyl; manganese; trifluoroacetic acid; cobalt(II) dibromide in pyridine; N,N-dimethyl-formamide T=50°C;
参考文献
Amatore, Muriel; Gosmini, Corinne; Perichon, Jacques
European Journal of Organic Chemistry, 2005 , # 6 p. 989 - 992
104-92-7
4-溴苯甲醚
+
78-08-0
乙烯基三乙氧基硅烷
→
反应条件
637-69-4
4-甲氧基苯乙烯
+
4356-69-8
1,1-二(对茴香基)乙烯
+
4705-34-4
4,4'-二甲氧基芪
反应条件
sodium hydroxide; poly(ethylene glycol) 2000; palladium diacetate in water T=150°C; Hiyama reaction; 3 h;
参考文献
Gordillo, Alvaro; De Jesus, Ernesto; Lopez-Mardomingo, Carmen
Chemical Communications, 2007 , # 39 p. 4056 - 4058
6303-59-9
1-((E)-2-溴乙烯基)-4-甲氧基苯
+
100-52-7
苯甲醛
→
反应条件
637-69-4
4-甲氧基苯乙烯
+
18684-94-1
4-甲氧基-反式-beta-氯苯乙烯
反应条件
copper(l) iodide; N,N-dimethylaminoacetic acid; [RuCl2Cp*]; caesium carbonate; lithium iodide in N,N-dimethyl-formamide T=120°C; P=760.051 Torr; 4 h; Inert atmosphereSealed tube; stereoselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 134, # 40 p. 16468 - 16471,4
6303-59-9
1-((E)-2-溴乙烯基)-4-甲氧基苯
+
100-52-7
苯甲醛
→
反应条件
637-69-4
4-甲氧基苯乙烯
+
136618-41-2
反应条件
copper(l) iodide; N,N-dimethylaminoacetic acid; [RuCl2Cp*]; caesium carbonate; potassium iodide in N,N-dimethyl-formamide T=120°C; P=760.051 Torr; 4 h; Inert atmosphereSealed tube; Reagent/catalyst; stereoselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 134, # 40 p. 16468 - 16471,4
104-94-9
对甲氧基苯胺
→
反应条件
637-69-4
4-甲氧基苯乙烯
反应条件
1: 4-methoxy-aniline With tetrafluoroboric acid; sodium nitrite in water T=0 - 5°C; Diazotization; 0.5 h; 2: potassium vinyl trifluoroborate With bis(tri-o-tolylphosphine)palladium acetate in methanol T=20°C; Arylation; 0.333333 h;
参考文献
Darses, Sylvain; Michaud, Guillaume; Genet, Jean-Pierre
European Journal of Organic Chemistry, 1999 , # 8 p. 1875 - 1883
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