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1: (E)-4-methoxyacetophenone tosylhydrazone With Mes2Mg; lithium chloride in tetrahydrofuran T=40°C; Shapiro reaction; 3 h; 2: N-methoxy-N-methyl-2,2-dimethyl-propamide in tetrahydrofuran T=40°C; 3: With water-d2 in tetrahydrofuran
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