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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
对氯碘苯
合成路线
（共 633 条）
637-87-6
对氯碘苯
+
108-98-5
硫酚
+
82102-37-2
→
反应条件
28122-82-9
反应条件
N,N-dicyclohexylmethylamine; sodium acetate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 T=85°C; 18 h; chemoselective reaction;
参考文献
Burhardt, Mia N.; Taaning, Rolf H.; Skrydstrup, Troels
Organic Letters, 2013 , vol. 15, # 4 p. 948 - 951
637-87-6
对氯碘苯
+
79099-07-3
N-叔丁氧羰基-4-哌啶酮
→
反应条件
235109-63-4
反应条件
1: 1-chloro-4-iodobenzene With n-butyllithium in tetrahydrofuran T=-78°C; 0.5 h; Inert atmosphere; 2: tert-butyl 4-oxo-piperidine-1-carboxylate in tetrahydrofuran T=-78°C; 1 h; Inert atmosphere;
参考文献
3-V BIOSCIENCES, INC.; OSLOB, Johan D.; MCDOWELL, Robert S.; JOHNSON, Russell; YANG, Hanbiao; EVANCHIK, Marc; ZAHARIA, Cristiana A.; CAI, Haiying; HU, Lily W.
Patent: WO2014/8197 A1, 2014 ;
Location in patent: Page/Page column 111; 112 ;
1453-58-3
3-甲基吡唑
+
637-87-6
对氯碘苯
→
反应条件
27301-77-5
反应条件
tripotassium phosphate monohydrate; MnCl2∙4H2O; (1S,2S)-1,2-diaminocyclohexane in water T=130°C; 48 h; chemoselective reaction;
参考文献
Teo, Yong-Chua; Yong, Fui-Fong; Poh, Chai-Yun; Yan, Yaw-Kai; Chua, Guan-Leong
Chemical Communications, 2009 , # 41 p. 6258 - 6260
637-87-6
对氯碘苯
+
106-53-6
→
反应条件
24535-57-7
反应条件
2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; copper(l) chloride in 1-methyl-pyrrolidin-2-one T=130°C; 2 h; Inert atmosphereSealed tube;
参考文献
Hoffmann-La Roche Inc.; Firooznia, Fariborz; Lin, Tai-An; Mertz, Eric; So, Sung-Sau; Sidduri, Achyutharao; Tilley, Jefferson Wright
Patent: US2013/225588 A1, 2013 ;
Location in patent: Paragraph 0224 ;
637-87-6
对氯碘苯
+
201230-82-2
+
536-74-3
+
100-63-0
→
反应条件
27293-95-4
反应条件
triethylamine in methanol P=760.051 Torr; 6 h; Schlenk technique;
参考文献
Li, Zelong; Liu, Jianhua; Huang, Zhiwei; Yang, Ying; Xia, Chungu; Li, Fuwei
ACS Catalysis, 2013 , vol. 3, # 5 p. 839 - 845
637-87-6
对氯碘苯
→
反应条件
27293-95-4
反应条件
1: 71 percent / diphenylphosphino ferrocene; Et3N / Pd(OAc)2 / tetrahydrofuran 2: ethanol / Heating View Scheme
参考文献
Bishop, Brian C.; Brands, Karel M. J.; Gibb, Andrew D.; Kennedy, Derek J.
Synthesis, 2004 , # 1 p. 43 - 52
→
反应条件
2491-90-9
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium carbonate in dimethyl sulfoxide T=120°C; 4 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 11, # 14 p. 3072 - 3075
288-47-1
+
637-87-6
对氯碘苯
→
反应条件
27149-26-4
反应条件
copper(l) iodide; palladium diacetate in N,N-dimethyl-formamide T=140°C; 40 h; regioselective reaction;
参考文献
Tani, Satoshi; Uehara, Takahiro N.; Yamaguchi, Junichiro; Itami, Kenichiro
Chemical Science, 2013 , vol. 5, # 1 p. 123 - 135
637-87-6
对氯碘苯
+
1864-94-4
→
反应条件
26459-51-8
反应条件
{(Pd{Fe(.eta.5-C5H5)(.eta.5-C5H3C(CH3)=NC6H4CH3-4)}(.mu.-Cl))2}; triethylamine; triphenylphosphine in N,N-dimethyl-formamide T=120°C; 23 h; Inert atmosphere;
参考文献
Chen, Guangwei; Leng, Yuting; Yang, Fan; Wang, Shiwei; Wu, Yangjie
Chinese Journal of Chemistry, 2013 , vol. 31, # 12 p. 1488 - 1494
637-87-6
对氯碘苯
→
反应条件
26018-88-2
反应条件
1: With sulfuric acid T=50 - 55°C; 2: With sodium periodate T=50 - 55°C; 3 h; 3: With potassium bromide in water
参考文献
Niu, Hong-Ying; Xia, Chao; Qu, Gui-Rong; Zhang, Qian; Jiang, Yi; Mao, Run-Ze; Li, De-Yang; Guo, Hai-Ming
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 14 p. 5039 - 5042
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