反应条件
1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran; toluene / 20 h / 20 °C / |Inert atmosphere
1.2: 20 - 50 °C / |Inert atmosphere
2.1: Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C / |Inert atmosphere
3.1: sodium dihydrogen phosphate dihydrate; 2-methyl-but-2-ene; sodium chlorite / water; tert-butyl alcohol / 2 h / 0 °C / |Inert atmosphere
4.1: hydrogen / water; methanol / 24 h / 20 °C / 3800.26 Torr
4.2: |Inert atmosphere
View Scheme
参考文献
Yang, Xiao-Fei; Ding, Chang-Hua; Li, Xiao-Hui; Huang, Jian-Qiang; Hou, Xue-Long; Dai, Li-Xin; Wang, Pin-Jie
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 8980 - 8985,6
Title/Abstract Full Text Show Details
Yang, Xiao-Fei; Ding, Chang-Hua; Li, Xiao-Hui; Huang, Jian-Qiang; Hou, Xue-Long; Dai, Li-Xin; Wang, Pin-Jie
Journal of Organic Chemistry, 2012 , vol. 77, # 20 p. 8980 - 8985
