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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
63715-12-8
合成路线
（共 9 条）
22516-18-3
+
124-63-0
甲烷磺酰氯
→
反应条件
63715-12-8
反应条件
in pyridine T=0°C; 48 h;
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
3197-68-0
2-(1-环己烯基)乙醇
→
反应条件
63715-12-8
反应条件
1: 71 percent / pyridine / 24 h / 0 - 5 °C 2: 54 percent / NaI / acetone / 24 h / Heating 3: 94 percent / NaCN / 72 h / 80 °C 4: 84 percent / KOH / ethanol; H2O / 18 h / 80 - 90 °C 5: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C 6: 73 percent / pyridine / 48 h / 0 °C View Scheme
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
53723-52-7
→
反应条件
63715-12-8
反应条件
1: 62 percent / LiAlH4 / diethyl ether / 3 h / 0 - 20 °C 2: 71 percent / pyridine / 24 h / 0 - 5 °C 3: 54 percent / NaI / acetone / 24 h / Heating 4: 94 percent / NaCN / 72 h / 80 °C 5: 84 percent / KOH / ethanol; H2O / 18 h / 80 - 90 °C 6: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C 7: 73 percent / pyridine / 48 h / 0 °C View Scheme
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
60-12-8
苯乙醇
→
反应条件
63715-12-8
反应条件
1: 48 percent / Li; PrNH2 2: 71 percent / pyridine / 24 h / 0 - 5 °C 3: 54 percent / NaI / acetone / 24 h / Heating 4: 94 percent / NaCN / 72 h / 80 °C 5: 84 percent / KOH / ethanol; H2O / 18 h / 80 - 90 °C 6: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C 7: 73 percent / pyridine / 48 h / 0 °C View Scheme
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
6975-71-9
1-环己烯乙腈
→
反应条件
63715-12-8
反应条件
1: 99 percent / 96 percent H2SO4 / 72 h / Heating 2: 62 percent / LiAlH4 / diethyl ether / 3 h / 0 - 20 °C 3: 71 percent / pyridine / 24 h / 0 - 5 °C 4: 54 percent / NaI / acetone / 24 h / Heating 5: 94 percent / NaCN / 72 h / 80 °C 6: 84 percent / KOH / ethanol; H2O / 18 h / 80 - 90 °C 7: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C 8: 73 percent / pyridine / 48 h / 0 °C View Scheme
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
27338-44-9
→
反应条件
63715-12-8
反应条件
1: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C 2: 73 percent / pyridine / 48 h / 0 °C View Scheme
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
13992-92-2
→
反应条件
63715-12-8
反应条件
1: 84 percent / KOH / ethanol; H2O / 18 h / 80 - 90 °C 2: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C 3: 73 percent / pyridine / 48 h / 0 °C View Scheme
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
82201-80-7
→
反应条件
63715-12-8
反应条件
1: 94 percent / NaCN / 72 h / 80 °C 2: 84 percent / KOH / ethanol; H2O / 18 h / 80 - 90 °C 3: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C 4: 73 percent / pyridine / 48 h / 0 °C View Scheme
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
136425-21-3
→
反应条件
63715-12-8
反应条件
1: 54 percent / NaI / acetone / 24 h / Heating 2: 94 percent / NaCN / 72 h / 80 °C 3: 84 percent / KOH / ethanol; H2O / 18 h / 80 - 90 °C 4: 98 percent / LiAlH4 / diethyl ether / 18 h / 20 °C 5: 73 percent / pyridine / 48 h / 0 °C View Scheme
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
