3,3-二甲基-4-戊烯酸甲酯合成路线 （共 12 条）
参考文献
ICI Australia Limited
Patent: US4374264 A1, 1983 ;
反应条件
sodium cyanide in water; dimethyl sulfoxide T=160°C;
参考文献
Trost, Barry M.; Braslau, Rebecca
Tetrahedron Letters, 1988 , vol. 29, # 11 p. 1231 - 1234
反应条件
B(C6F5)3 in methanol
反应条件
1: BSA / Mo(CO)6 / toluene / 100 °C 2: 60 percent / NaCN / dimethylsulfoxide; H2O / 160 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 29, # 11 p. 1231 - 1234
反应条件
oxygen T=100°C; P=7600 Torr; 4 h; catalyst: none, Cu(OAc)2; various temperatures and pressures; Product distribution;
参考文献
Tanaka, Mariko; Urata, Hisao; Fuchikami, Takamasa
Tetrahedron Letters, 1986 , vol. 27, # 27 p. 3165 - 3168
反应条件
1: 82 percent / lithium aluminium hydride
2: 79 percent / tributylphosphine, bromine / dimethylformamide / 2 h / Ambient temperature
View Scheme
参考文献
NIPPON SODA CO., LTD
Patent: US2012/225895 A1, 2012 ;
反应条件
tin(IV) chloride in dichloromethane
参考文献
Bayer Aktiengesellschaft
Patent: US4425282 A1, 1984 ;
反应条件
oxygen
T=100°C; P=7600 Torr; 4 h; catalyst: none, Cu(OAc)2; various temperatures and pressures; Product distribution;
参考文献
Tanaka, Mariko; Urata, Hisao; Fuchikami, Takamasa
Tetrahedron Letters, 1986 , vol. 27, # 27 p. 3165 - 3168
反应条件
1: With sodium hydroxide
5 h; Reflux;
2: With hydrogenchloride in water
参考文献
Zhu, Yaoping; Yeng, Xueyan; Fang, Xiang; Yang, Xianjin; Ye, Lingling; Cai, Wei; Zhang, Yan; Wu, Fanhong
Tetrahedron, 2011 , vol. 67, # 6 p. 1251 - 1257
反应条件
1: Saponification
2: oxalyl chloride / CH2Cl2 / 1.5 h / 20 °C
View Scheme
参考文献
Zhu, Yaoping; Yeng, Xueyan; Fang, Xiang; Yang, Xianjin; Ye, Lingling; Cai, Wei; Zhang, Yan; Wu, Fanhong
Tetrahedron, 2011 , vol. 67, # 6 p. 1251 - 1257
