8-氧代-3-氮杂双环[3.2.1]辛烷-3-羧酸叔丁酯合成路线 （共 2 条）
反应条件
palladium(II) oxide hydrate in ethyl acetate
T=20°C; P=2736.18 Torr;
参考文献
DAINIPPON SUMITOMO PHARMA CO., LTD.; MIZUNO, Kazuhiro; IKEDA, Junya; NAKAMURA, Takanori; IWATA, Masato; OTAKA, Hiromichi; GOTO, Nana
Patent: WO2012/169649 A1, 2012 ;
Location in patent: Page/Page column 207; 208 ;
WO 2012/169649 A1
反应条件
1: chloro-trimethyl-silane / acetonitrile / 51 h / 20 - 50 °C
2: palladium(II) oxide hydrate / ethyl acetate / 20 °C / 2736.18 Torr
View Scheme
参考文献
DAINIPPON SUMITOMO PHARMA CO., LTD.; MIZUNO, Kazuhiro; IKEDA, Junya; NAKAMURA, Takanori; IWATA, Masato; OTAKA, Hiromichi; GOTO, Nana
Patent: WO2012/169649 A1, 2012 ;
WO 2012/169649 A1
