N,N-二异丙基-1,3-丙二胺合成路线 (共 6 条)
反应条件
nickel T=105°C; P=51485.6 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 74, p. 2016
反应条件
hydrogen; platinum on activated charcoal
参考文献
Journal of Medicinal and Pharmaceutical Chemistry, , vol. 5, p. 823 - 835
反应条件
in water 1.) 0 deg C to ambient temperature (slowly), 2.) reflux, overnight;
参考文献
Denmark, Scott E.; Stadler, Heinz; Dorow, Roberta L.; Kim, Jung-Ho
Journal of Organic Chemistry, 1991 , vol. 56, # 17 p. 5063 - 5079
反应条件
(i) , (ii) H2, Raney-Ni; Multistep reaction;
参考文献
Journal of the Chemical Society [Section] B: Physical Organic, , p. 131 - 135
反应条件
in methanol T=47°C; 2 h;
参考文献
Mayr, Monika; Wurst, Klaus; Ongania, Karl-Hans; Buchmeiser, Michael R.
Chemistry - A European Journal, 2004 , vol. 10, # 5 p. 1256 - 1266
反应条件
triethylamine; phosphorus trichoride in benzene 2 h; Ambient temperature;
参考文献
Nifant'ev, E. E.; Zavalishina, A. I.; Orzhekovskaya, E. I.; Vasyanina, L. K.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 4.1 p. 816 - 820,720 - 723