6-氟-2(3氢)苯噻唑酮合成路线 (共 3 条)
反应条件
1: With copper(l) iodide; Na2S*9H2O in N,N-dimethyl-formamide T=80°C; Inert atmosphere; 2: With acetic acid in N,N-dimethyl-formamide T=130°C; 36 h; Inert atmosphere;
参考文献
Li, Jiaojiao; Zhang, Yihua; Jiang, Yongwen; Ma, Dawei
Tetrahedron Letters, 2012 , vol. 53, # 20 p. 2511 - 2513
参考文献
Dr. Karl Thomae Gesellschaft mit beschrankter Haftung
Patent: US4353919 A1, 1982 ;
反应条件
1: NaNO2, aq. HCl 2: aq. HCl View Scheme
参考文献
Farmaco, Edizione Scientifica, , vol. 32, p. 348 - 354