Boc-O-苄基-D-酪氨酸合成路线 (共 8 条)
反应条件
crown ether in N,N-dimethyl-formamide; benzene 4 h;
参考文献
Journal of Medicinal Chemistry, , vol. 25, # 1 p. 45 - 50
反应条件
triethylamine in water; acetone 4 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 48, # 40 p. 8601 - 8614
反应条件
1: 1) 2 N NaOH, CuSO4*5H2O, 2) aq. HCl / 1) MeOH 2: 68 percent / N(Et)3 / acetone; H2O / 4 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 48, # 40 p. 8601 - 8614
反应条件
1: 1) 2 N NaOH, CuSO4*5H2O, 2) aq. HCl / 1) MeOH 2: 68 percent / N(Et)3 / acetone; H2O / 4 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 48, # 40 p. 8601 - 8614
反应条件
sodium hydride in tetrahydrofuran; N,N-dimethyl-formamide Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Boger, Dale L.; Zhou, Jiacheng; Borzilleri, Robert M.; Nukui, Seiji; Castle, Steven L.
Journal of Organic Chemistry, 1997 , vol. 62, # 7 p. 2054 - 2069
反应条件
sodium hydride in tetrahydrofuran; N,N-dimethyl-formamide T=0 - 25°C; 10 h; Yield given;
参考文献
Boger, Dale L.; Zhou, Jiacheng
Journal of Organic Chemistry, 1996 , vol. 61, # 12 p. 3938 - 3939
反应条件
sodium hydride in tetrahydrofuran; N,N-dimethyl-formamide Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Boger, Dale L.; Zhou, Jiacheng; Borzilleri, Robert M.; Nukui, Seiji; Castle, Steven L.
Journal of Organic Chemistry, 1997 , vol. 62, # 7 p. 2054 - 2069
反应条件
1: NaH / tetrahydrofuran; dimethylformamide / 10 h / 0 - 25 °C 2: H2 / Pd-C / methanol / 25 °C View Scheme
参考文献
Boger, Dale L.; Zhou, Jiacheng
Journal of Organic Chemistry, 1996 , vol. 61, # 12 p. 3938 - 3939