3-甲基-5-硝基-1,2-苯异噁唑合成路线 （共 4 条）
反应条件
N-chloro-succinimide; potassium carbonate in tetrahydrofuran
T=20°C; 12 h; Inert atmosphere;
参考文献
Chen, Cheng-Yi; Andreani, Teresa; Li, Hongmei
Organic Letters, 2011 , vol. 13, # 23 p. 6300 - 6303
反应条件
potassium hydroxide in ethanol; dichloromethane
参考文献
BASF Aktiengesellschaft
Patent: US6355796 B1, 2002 ;
反应条件
sodium t-butanolate in tetrahydrofuran
Cooling with ice;
参考文献
Udd, Sandra; Jokela, Reija; Franzen, Robert; Tois, Jan
Tetrahedron Letters, 2010 , vol. 51, # 7 p. 1030 - 1033
反应条件
1: ammonia / methanol / 2 h / 20 °C / Inert atmosphere
2: N-chloro-succinimide; potassium carbonate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Chen, Cheng-Yi; Andreani, Teresa; Li, Hongmei
Organic Letters, 2011 , vol. 13, # 23 p. 6300 - 6303
