反应条件
1.1: 90 percent / benzylidene-bis(tricyclohexylphosphine)-dichlororuthenium / CH2Cl2 / 3 h / 23 °C
2.1: 97 percent / n-BuLi / tetrahydrofuran; hexane / 1.5 h / -78 - 23 °C
3.1: LiEt3BH / tetrahydrofuran / 0.75 h / -78 °C
3.2: 86 percent / tetrabutylammonium fluoride / tetrahydrofuran / 12 h / 23 °C
View Scheme
参考文献
Trzoss, Michael; Brimble, Margaret A.
Synlett, 2003 , # 13 p. 2042 - 2046
