n-butyllithium in diethyl ether T=-30°C;

(3,5-dioxa-4-phospha-cyclohepta[2,1-a;3,4-a']diphenyl-4-en)-dibenzo[b,f]azepine; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; C23H27F6NO4S2 in chloroform T=25°C; 24 h; Molecular sieve;