3-甲基-2-丁烯酸乙酯合成路线 （共 160 条）
参考文献
Courtot
Bulletin de la Societe Chimique de France, 1906 , vol. <3>35, p. 984
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Blaise; Courtot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1905 , vol. 140, p. 371
参考文献
Courtot
Bulletin de la Societe Chimique de France, 1906 , vol. <3>35, p. 984
Full Text Show Details
Blaise; Courtot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1905 , vol. 140, p. 371
参考文献
Matsui et al.
Journal of Vitaminology, 1958 , vol. 4, p. 190,192
反应条件
n-butyllithium in tetrahydrofuran; hexane from -78 deg C to r.t.;
参考文献
Smith, Amos B.; Visnick, Melean
Tetrahedron Letters, 1985 , vol. 26, # 32 p. 3757 - 3760
反应条件
1: 100 percent / EtONa / ethanol / 36 h / 20 - 50 °C 2: LiAlH4 / tetrahydrofuran / 1.5 h / Heating 3: 12.1 g / Na / liquid ammonia; diethyl ether / 1.5 h / -78 °C View Scheme
参考文献
Ohsugi, Shin-Ichi; Nishide, Kiyoharu; Node, Manabu
Tetrahedron, 2003 , vol. 59, # 11 p. 1859 - 1871
反应条件
1: N-bromosuccinimide, d'acide m-chloroperbenzoique / CCl4 2: 42 percent / H2SO4 / H2O 3: 45 percent / various solvent(s) / 15 h / Heating View Scheme
参考文献
Le Baut; Sparfel; Clairc; et al.
European Journal of Medicinal Chemistry, 1983 , vol. 18, # 5 p. 447 - 455
参考文献
Journal of Vitaminology, , vol. 4, p. 190,192
反应条件
1: 90 percent / SeO2 / aq. ethanol / 24 h / Heating 2: 72 percent / CaSO4, MnO2 / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Sisido,K. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 2286 - 2288
反应条件
1: 89 percent / NH3(gas) / ethanol / 22 h / 80 °C 2: 81 percent / CH2Cl2 / 18 h 3: 82 percent / aq. KOH / tetrahydrofuran / 18 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 34, # 2 p. 633 - 642
反应条件
AlCl3, aluminium chloride in dichloromethane 3 h; Inert atmosphereCoolingReflux;
参考文献
Sun, Chang-Liang; Fuerstner, Alois
Angewandte Chemie - International Edition, 2013 , vol. 52, # 49 p. 13071 - 13075
Angew. Chem., 2013 , vol. 125, # 49 p. 13309 - 13313,5
