3-甲基-2-丁烯酸乙酯合成路线 （共 160 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=130°C; 8 h;
参考文献
Kawase, Yoshiyuki; Yamaguchi, Seiji; Horita, Hisanori; Takeno, Junko; Kameyama, Hideaki
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 4 p. 1153 - 1155
反应条件
1: diisobutylaluminium hydride / hexane; toluene / 0.08 h / -78 °C / |Inert atmosphere
2: tributylphosphine / tetrahydrofuran / 12 h / 0 - 25 °C / |Inert atmosphere
3: 3-chloro-benzenecarboperoxoic acid / chloroform; water / 1.33 h / 0 °C
View Scheme
参考文献
Kimura, Tsutomu; Kobayashi, Gen; Ishigaki, Masashi; Inumaru, Mio; Sakurada, Jo; Satoh, Tsuyoshi
Synthesis (Germany), 2012 , vol. 44, # 23 art. no. SS-2012-F0694-OP, p. 3623 - 3632
反应条件
in acetone; tert-butyl alcohol
Irradiation;
参考文献
Smith,A.B. et al.
Tetrahedron Letters, 1975 , p. 4225 - 4228
反应条件
lithium diisopropyl amide in tetrahydrofuran
1.) -78 deg C, 1 h, 2.) -78 deg C -> room temperature, 1 h;
参考文献
Smith,A.B.; Toder,B.H.; Branca,S.J.
Journal of the American Chemical Society, 1981 , vol. 103, p. 1996
反应条件
benzophenone in benzene
24 h; Irradiation;
参考文献
Cerfontain, Hans; Noort, Paul C. M. van
Synthesis, 1980 , # 6 p. 490 - 492
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; lithium diisopropyl amide
参考文献
Overman, Larry E.; Renaldo, Alfred F.
Tetrahedron Letters, 1983 , vol. 24, # 35 p. 3757 - 3760
反应条件
lithium diisopropyl amide in tetrahydrofuran
T=-78 - 10°C;
参考文献
Bloodworth; Bothwell, Brian D.; Collins, Andrew N.; Maidwell, Nicola L.
Tetrahedron Letters, 1996 , vol. 37, # 11 p. 1885 - 1888
反应条件
tetra-n-butylammonium perchlorate in N,N-dimethyl-formamide
T=-15°C; (electrolysis);
参考文献
Thomas,H.G.; Thoennessen,F.
Chemische Berichte, 1979 , vol. 112, p. 2786 - 2797
反应条件
tetra-n-butylammonium perchlorate in N,N-dimethyl-formamide
T=-15°C; (electrolysis);
参考文献
Thomas,H.G.; Thoennessen,F.
Chemische Berichte, 1979 , vol. 112, p. 2786 - 2797
反应条件
selenium(IV) oxide in ethanol
24 h; Heating;
参考文献
Curley, Robert W.; Ticoras, Christ J.
Journal of Organic Chemistry, 1986 , vol. 51, # 2 p. 256 - 258
