3-甲基-2-丁烯酸乙酯合成路线 (共 160 条)
反应条件
T=35°C; P=6750540 Torr; 24 h;
参考文献
Isaacs, Neil S.; El-Din, Ghazi Najim
Tetrahedron Letters, 1987 , vol. 28, # 19 p. 2191 - 2192
反应条件
triethylamine; phosphonic acid diethyl ester T=80°C; 30 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 51, # 14 p. 2830 - 2832
反应条件
tri-n-butyl-antimony T=130°C; 6 h;
参考文献
Huang, Yao-Zeng; Chen, Chen; Shen, Yanchang
Journal of Organometallic Chemistry, 1989 , vol. 366, p. 87 - 94
反应条件
1: triphenylphosphine dibromide / 0.25 h / Ambient temperature 2: 2-oxo-3-trimethyltetrahydro-1,3-oxazole / 0.25 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 8 p. 684 - 686
反应条件
piperidine in tetrahydrofuran
参考文献
Journal of Organometallic Chemistry, , vol. 96, p. 163 - 168
反应条件
in dichloromethane T=15°C; 15 h; Yield given;
参考文献
Synthesis, , # 8 p. 684 - 686
反应条件
sodium iodide T=60°C;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , p. 77
Zhurnal Obshchei Khimii, , vol. 4, p. 1050
Chem. Zentralbl., , vol. 105, # I p. 3212
反应条件
boric acid T=0 - 10°C; und anschliessenden Kochen;
反应条件
boron trifluoride diethyl etherate in diethyl ether
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 85, p. 929 - 951
反应条件
amalgamated zinc; benzene
参考文献
Journal of Organic Chemistry, , vol. 16, p. 728,729