N-(2-氯苯基)-4-甲基苯磺酰胺合成路线 （共 15 条）
反应条件
potassium carbonate in water
5 h; Reflux;
参考文献
Azarifar, Davood; Soleimanei, Fatemeh
RSC Advances, 2014 , vol. 4, # 24 p. 12119 - 12126
反应条件
sodium peroxodisulphate; N-chloro-succinimide; trifluorormethanesulfonic acid; palladium diacetate in 1,2-dichloro-ethane
T=60°C; 1 h; Sealed tube; regioselective reaction;
参考文献
Sun, Xiuyun; Shan, Gang; Sun, Yonghui; Rao, Yu
Angewandte Chemie - International Edition, 2013 , vol. 52, # 16 p. 4440 - 4444
Angew. Chem., 2013 , vol. 125, # 16 p. 4536 - 4540,5
反应条件
1: N-chloro-succinimide; tetrabutyl-ammonium chloride; water / acetonitrile / 0 °C
2: acetonitrile / 1 h / 20 °C
View Scheme
参考文献
Veisi, Hojat; Ghorbani-Vaghei, Ramin; Hemmati, Saba; Mahmoodi, Jafar
Synlett, 2011 , # 16 art. no. B11411ST, p. 2315 - 2320
反应条件
1: cyanic acid sodium salt / water / 0.17 h / |Reflux
2: potassium carbonate / water / 5 h / |Reflux
View Scheme
参考文献
Azarifar, Davood; Soleimanei, Fatemeh
RSC Advances, 2014 , vol. 4, # 24 p. 12119 - 12126
反应条件
1: 1,3-Dichloro-5,5-dimethyl-2,4-imidazolidinedione; water; N-benzyl-N,N,N-trimethyl-ammonium chloride / acetonitrile / 0.5 h / 0 °C
2: acetonitrile / 0.5 h / 20 °C
View Scheme
参考文献
Veisi, Hojat
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 2 p. 383 - 386
