Chambers, R. F.; Scherer, P. C.
Journal of the American Chemical Society, 1926 , vol. 48, p. 1054 - 1062
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.2.1.7.4, page 115 - 118
Na in tetrahydrofuran; ammonia
byproducts: NaCl; NH3 (liquid); Ph2SnCl2 soln. (THF) added dropwise to soln. of Na (2 equiv.) (liq. NH3)at 200 K at stirring (in the dark); NH3 removed in N2 flow by warming to room temp., THF evapd. at room temp. in vac., residue dissolved in CH2Cl2, ppt. filtered off, solvent evapd., residue dried in vac.; elem. anal.;
参考文献
Trummer, Markus; Zemp, Jerome; Sax, Cedric; Smith, Paul; Caseri, Walter
Journal of Organometallic Chemistry, 2011 , vol. 696, # 19 p. 3041 - 3049
in further solvent(s)
byproducts: C6H5(2)H; C6H5D, heating at 50°C for 22 h;
参考文献
Bhattacharyya, Koyel X.; Akana, Jennifer A.; Laitar, David S.; Berlin, Jacob M.; Sadighi, Joseph P.
Organometallics, 2008 , vol. 27, # 12 p. 2682 - 2684
Bhattacharyya, Koyel X.; Akana, Jennifer A.; Laitar, David S.; Berlin, Jacob M.; Sadighi, Joseph P.
Organometallics, 2008 , vol. 27, # 12 p. 2682 - 2684
