反应条件
hydrogenchloride in tetrahydrofuran mixing of Zr-complex with Li-salt in THF (molar ratio 1:1, -78°C, 1 h), rise of temp. to 25°C (over 1 h); gas liquid chromy. after quenching with 2 N HCl;
参考文献
Negishi, Ei-ichi; Akiyoshi, Kazunari; O'Connor, Brian; Takagi, Kentaro; Wu, Guangzhong
Journal of the American Chemical Society, 1989 , vol. 111, # 8 p. 3089 - 3091
